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In many processes utilizing chemical compounds, it is often desirable to separate certain components from others. For example, in a chemical plant where ammonia is manufactured, the impurities may include hydrogen cyanide, carbon dioxide, carbon monoxide, oxygen, nitrogen and the like. It is highly desirable to recover the ammonia. If the ammonia contains only minor amounts of these impurities, the ammonia may be produced as a by-product in one of the manufacturing steps. If there is too much of one or more impurities in the ammonia, a modification of the reaction may be required to produce the desired product.

On the other hand, separation of ammonia from impurities is a problem if the impurities are present in a large amount. Such impurities may be removed from the ammonia to make the product sellable, or the impurities may be removed from the ammonia because they are valuable and it is desirable to recover these impurities. For example, the impurities may be used as a source of energy for other processes, or they may be sold.

One method of separating the ammonia from its impurities is by using a distillation column. In such a column, one or more reboilers heat the entire column to heat the desired component. The desired product is recovered at the top of the column, and other components are recovered at lower levels.

Because distillation columns operate on principles well-known in the art, there is no further description here. However, it is noted that the distillation column is well-suited to the separation of the ammonia from its impurities. Separation efficiency may be improved by increasing the temperature of the liquid. However, many chemicals decompose when subjected to high temperatures. Thus, most distillation columns are designed with an operating range which is limited to the temperature at which the material to be separated does not decompose. For example, distillation columns may be operated in a range of about 200.degree. F. to about 600.degree. F. Thus, even if the reboiler is heated to a temperature of 1000.degree. F., the ammonia is only heated to a temperature of about 200.degree. F.

Another way of improving separation efficiency is to mix the liquid in the distillation column. For example, the amount of heat energy required to produce a given amount of a particular component may 0b46394aab

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Vikalp 2 720p Download Movies